[1] MAO TingMAO LeZHANG PingZHANG Yong,.Preparation of Tu Mu Xiang lactone and Iso Tu MuXiang lactone in Mongolian Medicine Tu Mu Xiangby Silver Nitrate Silica Gel Chromatography [J]. Modern Traditional Chinese Medicine, 2024, (03): 94-98. [doi: 10.13424/j.cnki.mtcm.2024.03.018]
Preparation of Tu Mu Xiang lactone and Iso Tu MuXiang lactone in Mongolian Medicine Tu Mu Xiangby Silver Nitrate Silica Gel Chromatography
- Article number:
- 1672-0571(2024)03-0094-05
- Keywords:
- Key words:Silver nitrate silica gel chromatography; Tu Tu Xiang lactone; Iso Tu Mu Xiang lactone
- ZTFLH:
- R93
- Code:
- A
- Abstract:
- Abstract：Objective To explore the preparation methods of Tu Mu Xiang lactone and Iso Tu Mu Xiang lactone in Mongolian medicine.Methods The method was prepared using silver nitrate silica gel chromatography.Results As a result，two crystalline compounds with excellent color and large weight were obtained，and identified as Tu Mu Xiang lactone and Iso Tu Mu Xiang lactone based on their physical and chemical properties and spectroscopic techniques.Conclusion Silver nitrate silica gel chromatography can achieve satisfactory separation of Tu Mu Xiang lactone and Iso Tu Mu Xiang lactone，with high yield，high purity，and simple operation.It is an efficient and rapid preparation method，providing accurate and reliable reference materials for the widespread application of Tu Mu Xiang lactone and Iso Tu Mu Xiang lactone.
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基金项目：国家自然科学基金地区项目(81460651)